Subjek penelitian pada penelitian ini adalah siswa kelas XI IPA SMAN 1 Surakarta dan SMAN Sragen Bilingual Boarding School tahun ajaran 2013/2014. ABSTRAK Penelitian ini bertujuan untuk mengembangkan instrumen penilaian Two-tier Multiple Choice yang memiliki validitas, reliabilitas, tingkat kesukaran, daya pembeda dan indeks pengecoh yang memenuhi kriteria sebagai suatu soal yang baik dan mengembangkan instrumen Two-tier Multiple Choice pada materi kelarutan dan hasil kali kelarutan menjadi instrumen penilaian yang mampu mengukur keterampilan berpikir tingkat tinggi.Penelitian ini merupakan penelitian pengembangan yang terdiri dari analisis kebutuhan dan penelitian awal, perencanaan, pengembangan bentuk awal produk, revisi dan uji lapangan awal, revisi dan uji lapangan utama, dan revisi dan uji pelaksanaan lapangan.
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